Solvent-Free Synthesis Of Novel Phthalocyanines Containing Triazole Derivatives Under Microwave Irradiation

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Bodur O., Özil M., Kahveci B.

IUPAC 2013 – 44th World Chemistry Congress, İstanbul, Türkiye, 11 - 16 Ağustos 2013, cilt.2, ss.1109, (Özet Bildiri)

  • Yayın Türü: Bildiri / Özet Bildiri
  • Cilt numarası: 2
  • Basıldığı Şehir: İstanbul
  • Basıldığı Ülke: Türkiye
  • Sayfa Sayıları: ss.1109
  • Açık Arşiv Koleksiyonu: AVESİS Açık Erişim Koleksiyonu
  • Süleyman Demirel Üniversitesi Adresli: Evet

Özet

Recently, much effort has been dedicated to the microwave assisted synthesis of metal-free and metallophthalocyanines [1]. In addition, there have been several incidences reported of the synthesis of unsubstituted, and some substituted, metallophthalocyanines using microwave irradiation under solvent free conditions [2,3].

A fast and effective procedure was developed for the synthesis of bulky substituted metal-free phthalocyanines and metallophthalocyanines. The present procedure described in this paper demonstrated that microwave processing combined with solvent-free condition leads to shorter reaction time, higher yield, a clean reaction product and easier workup than classical thermal processing [4].