Synthesis of ethane-1, 2-bis(thio-R-glyoximes) and their complexes with some transition metals


Sevindir H.

SYNTHESIS AND REACTIVITY IN INORGANIC AND METAL-ORGANIC CHEMISTRY, vol.30, no.1, pp.183-190, 2000 (Journal Indexed in SCI) identifier identifier

  • Publication Type: Article / Article
  • Volume: 30 Issue: 1
  • Publication Date: 2000
  • Doi Number: 10.1080/00945710009351756
  • Title of Journal : SYNTHESIS AND REACTIVITY IN INORGANIC AND METAL-ORGANIC CHEMISTRY
  • Page Numbers: pp.183-190

Abstract

Two new tetra-oximes, ethane-1,2-bis(thio-(p) under bar-nitrophenylglyoxime), [(LH4)-H-1], and ethane-1,2-bis(thio-(m) under bar-nitrophenylglyoxime), [(LH4)-H-2], have been synthesized from <(anti)under bar>-(p) under bar-nitrophenylchloroglyoxime or (m) under bar-nitrophenylchloroglyoxime and 1,2-ethanedithiol. Their polymeric complexes with Ni(II), Cu(II) and Co(III) ions have been prepared. H-1 NMR IR spectra and elemental analyses data are given.