SYNTHESIS AND COMPLEX-FORMATION OF SUBSTITUTED AMINOPHENYLGLYOXIMES OF UNSYMMETRICAL VIC-DIOXIMES


SEVINDIR H.

SYNTHESIS AND REACTIVITY IN INORGANIC AND METAL-ORGANIC CHEMISTRY, cilt.24, ss.953-961, 1994 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 24 Konu: 6
  • Basım Tarihi: 1994
  • Doi Numarası: 10.1080/00945719408001314
  • Dergi Adı: SYNTHESIS AND REACTIVITY IN INORGANIC AND METAL-ORGANIC CHEMISTRY
  • Sayfa Sayıları: ss.953-961

Özet

anti-Chlorophenylglyoxime(CPGH2) has been synthesized by chlorination of anti-phenylglyoxime. The reaction of CPGH2 with P-chloroaniline, o-chloraniline and m-chloroaniline in ethanol between -10-degrees-C and -15-degrees-C gives unsymmetrical vic-dioximes, namely, p-chloroanilinophenylglyoxime (p-CAPGH2), o-chloroanilinophenylglyoxime (o-CAPGH2), m-chloroanilino-phenylglyoxime (m-CAPGH2). H-1-NMR, mass, IR spectra and elemental analyses data are given.